sodium salt of p-bromobenzoylacetaldehyde

Base Information

• Chemical Name: sodium salt of p-bromobenzoylacetaldehyde
• CAS No.: 53073-03-3
• Molecular Formula: C₉H₆BrO₂*Na
• Molecular Weight: 249.039
• Mol file: 53073-03-3.mol

Synonyms:sodium salt of p-bromobenzoylacetaldehyde

Chemical Property of sodium salt of p-bromobenzoylacetaldehyde

Chemical Property:

Purity/Quality:

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Technology Process of sodium salt of p-bromobenzoylacetaldehyde

There total 1 articles about sodium salt of p-bromobenzoylacetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ sodium salt of p-bromobenzoylacetaldehyde (53073-03-3)

Guidance literature:

4-Brom-acetophenon, Ethylformiat, Na /Ae.;

Reference yield: 57.0%

Cyanothioacetamide (7357-70-2) + sodium salt of p-bromobenzoylacetaldehyde (53073-03-3) → 6-(4-Brom-phenyl)-2-thioxo-1,2-dihydro-pyridin-3-carbonitril (118947-84-5)

Guidance literature:

With acetic acid; In ethanol; Heating;

DOI:10.1007/BF00475603

Reference yield:

sodium salt of p-bromobenzoylacetaldehyde (53073-03-3) → N-[5-(4-Bromo-phenyl)-4,5-dihydro-isoxazol-5-yl]-hydroxylamine (121557-14-0) + p-bromobenzoylacetaldehyde dioxime, anti,anti (Z,Z) isomer (121557-13-9) + p-bromobenzoylacetaldehyde dioxime, syn,anti (E,Z) isomer (121557-12-8)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride; In water; at 3 - 5 ℃; for 12h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Downstream raw materials:

1-(4-bromo-phenyl)-2-diazo-ethanone

Bis<2-(4-brombenzoyl)vinyl>-aether

5-(4-Bromo-phenyl)-4,5-dihydro-isoxazol-5-ol

Phosphoric acid (Z)-3-(4-bromo-phenyl)-3-oxo-propenyl ester diphenyl ester