benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

Base Information

Chemical Name:benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite
CAS No.:945491-75-8
Molecular Formula:C₄₈H₉₀NO₅P
Molecular Weight:792.22
Hs Code.:

Synonyms:benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

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Chemical Property of benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

Chemical Property:

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Technology Process of benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

There total 5 articles about benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 945491-74-7
(S)-2-(hexadecyloxy)-3-hydroxypropyl palmitate

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 945491-75-8
benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

Guidance literature:: With 1H-tetrazole; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jo070639m

Reference yield:

: 945491-72-5
1-O-allyl-3-O-benzyl-2-O-hexadecyl-sn-glycerol

: 945491-75-8
benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / N,N'-dimethylbarbituric acid / Pd(PPh₃)4 / tetrahydrofuran / 40 h / 90 °C

2: 96 percent / pyridine / CH₂Cl₂ / 12 h / 20 °C

3: 99 percent / H₂; acetic acid / Pd(OH)2/C / ethanol / 14 h

4: 96 percent / 1H-tetrazole / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 1H-tetrazole; 1,3-dimethylbarbituric acid; hydrogen; acetic acid; palladium dihydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo070639m

Reference yield:

: 573673-85-5
(R)-3-(benzyloxy)-2-(hexadecyloxy)propan-1-ol

: 945491-75-8
benzyl (1-O-hexadecanoyl-2-O-hexadecyl-sn-glycero)diisopropylphosphoramidite

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / pyridine / CH₂Cl₂ / 12 h / 20 °C

2: 99 percent / H₂; acetic acid / Pd(OH)2/C / ethanol / 14 h

3: 96 percent / 1H-tetrazole / CH₂Cl₂ / 1 h / 20 °C

With pyridine; 1H-tetrazole; hydrogen; acetic acid; palladium dihydroxide; In ethanol; dichloromethane;
DOI:10.1021/jo070639m