dimethyl 4-methoxy-1,3-phenylenediurethane

Base Information

• Chemical Name: dimethyl 4-methoxy-1,3-phenylenediurethane
• CAS No.: 1075727-38-6
• Molecular Formula: C₁₁H₁₄N₂O₅
• Molecular Weight: 254.243
• Mol file: 1075727-38-6.mol

Synonyms:dimethyl 4-methoxy-1,3-phenylenediurethane

Chemical Property of dimethyl 4-methoxy-1,3-phenylenediurethane

Chemical Property:

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Technology Process of dimethyl 4-methoxy-1,3-phenylenediurethane

There total 1 articles about dimethyl 4-methoxy-1,3-phenylenediurethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methanol (67-56-1) + formyl radical (2597-44-6) + 2,4-dinitroanisole (119-27-7) → dimethyl 4-methoxy-1,3-phenylenediurethane (1075727-38-6)

Guidance literature:

With 1,10-Phenanthroline; [trihexyl(tetradecyl)phosphonium hexafluorophosphate]; palladium dichloride; at 135 ℃; for 24h; under 10343.2 Torr;

DOI:10.1021/ol802096x

upstream raw materials:

methanol

formyl radical

2,4-dinitroanisole