N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

Base Information

Chemical Name:N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride
CAS No.:1372879-79-2
Molecular Formula:C₃₄H₄₆BrN₃O₆
Molecular Weight:672.66
Hs Code.:

Synonyms:N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

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Chemical Property of N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

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Technology Process of N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

There total 1 articles about N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83204-68-6
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride

: 1372879-79-2
N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 5 h / Reflux

2: ethyl methyl ether / 8 h / 120 °C

With acetic acid; In ethyl methyl ether;
DOI:10.1039/c1dt10679a

Reference yield: 94.0%

: 1372879-79-2
N,N'-di-(2-ethylhexan-1-amine)-2-(diethyleneglycolamino)-6-bromonaphthalene-1,4,5,8-tetra-carboxydianhydride

: 87199-17-5
4-formylphenylboronic acid,

: 1416251-77-8
C₄₁H₅₁N₃O₇

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; for 12h; Inert atmosphere; Heating; Darkness;
DOI:10.1016/j.dyepig.2012.09.008