Technology Process of C8H7FN2O
There total 6 articles about C8H7FN2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C10H9FN2O2;
With
hydrogenchloride;
In
ethanol; water;
for 1h;
Reflux;
With
sodium hydrogencarbonate;
In
water;
pH=7 - 8;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine; diphenylphosphoranyl azide / toluene / 2 h / 20 °C
1.2: 2 h / Reflux
2.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C
2.2: pH 8
3.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 20 °C
4.1: 1 h / 20 °C
5.1: N,N-dimethyl-formamide / 145 °C / Inert atmosphere
6.1: hydrogenchloride / ethanol; water / 1 h / Reflux
6.2: pH 7 - 8
With
hydrogenchloride; N-Bromosuccinimide; diphenylphosphoranyl azide; triethylamine; trifluoroacetic acid;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 20 °C
2.1: 1 h / 20 °C
3.1: N,N-dimethyl-formamide / 145 °C / Inert atmosphere
4.1: hydrogenchloride / ethanol; water / 1 h / Reflux
4.2: pH 7 - 8
With
hydrogenchloride; N-Bromosuccinimide;
In
ethanol; water; N,N-dimethyl-formamide;