bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

Base Information

Chemical Name:bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane
CAS No.:1217308-87-6
Molecular Formula:C₂₁H₈Cl₁₂O
Molecular Weight:701.73
Hs Code.:

Synonyms:bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

Suppliers and Price of bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

Chemical Property:

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Technology Process of bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

There total 1 articles about bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.7%

: 75-21-8,99932-75-9
oxirane

: 105633-26-9
Tris<2,3,5,6-tetrachlorophenyl>methane

: 1217308-87-6
bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

: 1217309-01-7
bis[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]-[2,3,5,6-tetrachloro-phenyl]methane

: 1217309-02-8
tri[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

Guidance literature:: Tris<2,3,5,6-tetrachlorophenyl>methane; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 ℃;

oxirane; In tetrahydrofuran; diethyl ether; at 20 ℃; Cooling;
DOI:10.1016/j.bmc.2009.11.034

Reference yield: 97.7%

: 136918-14-4,85-41-6
phthalimide

: 1217308-87-6
bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

: 1217308-88-7
bis(2,3,5,6-tetrachlorophenyl)-[4-(2-phthalimidoetheyl)-2,3,5,6-tetrachlorophenyl]methane

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmc.2009.11.034

Reference yield: 70.2%

: 1217308-87-6
bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane

: 541-41-3
chloroformic acid ethyl ester

: 1217308-96-7
bis[2,3,5,6-tetrachloro-4-ethoxycarbonyl-phenyl]-[4-(2-ethoxycarbonyloxy-ethyl)-2,3,5,6-tetrachloro-phenyl]methane

Guidance literature:: bis[2,3,5,6-tetrachlorophenyl]-[4-(2-hydroxyethyl)-2,3,5,6-tetrachlorophenyl]methane; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at -78 ℃;

chloroformic acid ethyl ester; In tetrahydrofuran; at -20 ℃;
DOI:10.1016/j.bmc.2009.11.034