tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate
CAS No.:1610591-35-9
Molecular Formula:C₂₃H₂₉Cl₃N₄O₄
Molecular Weight:531.867
Hs Code.:

Synonyms:tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

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Technology Process of tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

There total 3 articles about tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610418-21-7
tert-butyl 4-(5-amino-4-methyl-1-phenyl-1H-pyrazol-3-yl)piperidine-1-carboxylate

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 1610591-35-9
tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

Guidance literature:: With sodium hydroxide; In water; ethyl acetate; at 0 - 20 ℃; for 16.17h;

Reference yield:

: 124443-68-1
1-tert-Butyl 4-methyl piperidine-1,4-dicarboxylate

: 1610591-35-9
tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

1.2: -76 - 20 °C

2.1: ethanol / 16 h / Reflux

3.1: sodium hydroxide / ethyl acetate; water / 16.17 h / 0 - 20 °C

With sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; water; ethyl acetate;

Reference yield:

: 1610454-97-1
tert-butyl 4-(2-cyanopropanoyl)piperidine-1-carboxylate

: 1610591-35-9
tert-butyl 4-(4-methyl-1-phenyl-5-((2,2,2-trichloroethoxy)carbonylamino)-1H-pyrazol-3-yl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 16 h / Reflux

2: sodium hydroxide / ethyl acetate; water / 16.17 h / 0 - 20 °C

With sodium hydroxide; In ethanol; water; ethyl acetate;