methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

Base Information

Chemical Name:methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate
CAS No.:96186-29-7
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

Synonyms:methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

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Chemical Property of methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

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Technology Process of methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

There total 3 articles about methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 159002-15-0,62234-36-0
N^α-benzyloxycarbonyl-N^β-tert-butyloxycarbonyl-D-2,3-diaminopropionic acid

: 96186-29-7
methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethylmorpholine / ethyl acetate / 1 h / 0 °C

2: diethyl ether / 13 h / 0 - 20 °C

3: silver benzoate, triethylamine / 4 h / Ambient temperature

With N-ethylmorpholine;; silver benzoate; triethylamine; In diethyl ether; ethyl acetate;
DOI:10.1021/jm00391a030

Reference yield:

: 91289-64-4
C₁₉H₂₆N₂O₈

: 96186-29-7
methyl D-3-<(benzyloxycarbonyl)amino>-4-<(tert-butoxycarbonyl)amino>butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 13 h / 0 - 20 °C

2: silver benzoate, triethylamine / 4 h / Ambient temperature

With silver benzoate; triethylamine; In diethyl ether;
DOI:10.1021/jm00391a030