Technology Process of C14H15N5
There total 3 articles about C14H15N5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammomium bromide; sodium hydroxide;
In
water;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/co400034x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: phosphorus tribromide / dichloromethane / 0 - 20 °C
2: sodium azide / dimethyl sulfoxide / 1 h / 80 °C
3: tetrabutylammomium bromide; sodium hydroxide / water / 24 h / 20 °C / Inert atmosphere
With
sodium azide; tetrabutylammomium bromide; phosphorus tribromide; sodium hydroxide;
In
dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/co400034x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / dimethyl sulfoxide / 1 h / 80 °C
2: tetrabutylammomium bromide; sodium hydroxide / water / 24 h / 20 °C / Inert atmosphere
With
sodium azide; tetrabutylammomium bromide; sodium hydroxide;
In
water; dimethyl sulfoxide;
DOI:10.1021/co400034x