methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Base Information

Chemical Name:methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether
CAS No.:1155975-78-2
Molecular Formula:C₂₃H₂₀N₂O
Molecular Weight:340.425
Hs Code.:

Synonyms:methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Suppliers and Price of methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

There total 3 articles about methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1093116-12-1
2-((1H-indol-3-yl)methyl)aniline

: 123-11-5
4-methoxy-benzaldehyde

: 1155975-78-2
methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.666667h;
DOI:10.1002/ejoc.200801201

Reference yield:

: 120-72-9
indole

: 1155975-78-2
methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1,2-dichloro-ethane / 1.5 h / 80 °C / Inert atmosphere

2: 1,2-dichloro-ethane / 20 °C

With trifluoroacetic acid; In 1,2-dichloro-ethane; 2: |Pictet-Spengler Synthesis;
DOI:10.1002/ejoc.201300100

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 1155975-78-2
methyl 4-(5,6,7,12-tetrahydroindolo[2,3-c][1]benzazepine-6-yl)phenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 1,2-dichloro-ethane / 1.5 h / 80 °C / Inert atmosphere

2: 1,2-dichloro-ethane / 20 °C

With trifluoroacetic acid; In 1,2-dichloro-ethane; 2: |Pictet-Spengler Synthesis;
DOI:10.1002/ejoc.201300100