C₁₉H₁₅BrN₂O₅S

Base Information

Chemical Name:C₁₉H₁₅BrN₂O₅S
CAS No.:1251582-25-8
Molecular Formula:C₁₉H₁₅BrN₂O₅S
Molecular Weight:463.308
Hs Code.:

C<sub>19</sub>H<sub>15</sub>BrN<sub>2</sub>O<sub>5</sub>S

Synonyms:C₁₉H₁₅BrN₂O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₁₅BrN₂O₅S

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Technology Process of C₁₉H₁₅BrN₂O₅S

There total 6 articles about C₁₉H₁₅BrN₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1251582-22-5
C₁₈H₁₃BrN₂O₃

: 124-63-0
methanesulfonyl chloride

: 1251582-25-8
C₁₉H₁₅BrN₂O₅S

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1251582-25-8
C₁₉H₁₅BrN₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / acetone / 16 h / 75 °C

1.2: 0.25 h / 65 °C

2.1: potassium carbonate / toluene / 16 h / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C

3.2: 2 h / 20 - 90 °C

4.1: ammonium acetate / 2 h / 140 °C

4.2: pH 8 / Heating

5.1: triethylamine / dichloromethane / 1 h / 20 °C

With ammonium acetate; sodium hydride; sodium carbonate; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: C₁₅H₁₀BrNO₂

: 1251582-25-8
C₁₉H₁₅BrN₂O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / toluene / 16 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C

2.2: 2 h / 20 - 90 °C

3.1: ammonium acetate / 2 h / 140 °C

3.2: pH 8 / Heating

4.1: triethylamine / dichloromethane / 1 h / 20 °C

With ammonium acetate; sodium hydride; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;