6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

Base Information

Chemical Name:6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide
CAS No.:1571031-72-5
Molecular Formula:C₁₅H₁₂F₃N₃O₄
Molecular Weight:355.273
Hs Code.:

Synonyms:6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

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Chemical Property of 6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

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Technology Process of 6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

There total 1 articles about 6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 175277-18-6
4-trifluoromethoxybenzoyl hydrazine

: 38116-61-9
6-Methylpyrid-2-one-3-carboxylic Acid

: 1571031-72-5
6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

Guidance literature:: With 2-(1H-9-azabenzotriazol-1-yl)-1,1,3,3-tetramethyluroniumhexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield: 84.0%

: 1571031-72-5
6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

: 1571031-76-9
6-methyl-3-(5-(4-(trifluoromethoxy)phenyl)-1,3,4-oxadiazol-2-yl)pyridin-2(1H)-one

Guidance literature:: With Burgess Reagent; In tetrahydrofuran; at 60 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1571031-72-5
6-methyl-2-oxo-N'-(4-(trifluoromethoxy)benzoyl)-1,2-dihydropyridine-3-carbohydrazide

: 1571031-80-5
1-((2-chloropyridin-4-yl)methyl)-6-methyl-3-(5-(4-(trifluoromethoxy)phenyl)-1,3,4-oxadiazol-2-yl)pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Burgess Reagent / tetrahydrofuran / 1 h / 60 °C / Microwave irradiation

2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 16 h / 65 °C

With Burgess Reagent; caesium carbonate; sodium iodide; In tetrahydrofuran; N,N-dimethyl-formamide;