1,3-dimethyl-2-dimethylaminodiazaborinane

Base Information

Chemical Name:1,3-dimethyl-2-dimethylaminodiazaborinane
CAS No.:3693-07-0
Molecular Formula:C₇H₁₈BN₃
Molecular Weight:155.051
Hs Code.:

Synonyms:1,3-dimethyl-2-dimethylaminodiazaborinane

Suppliers and Price of 1,3-dimethyl-2-dimethylaminodiazaborinane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-dimethyl-2-dimethylaminodiazaborinane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-dimethyl-2-dimethylaminodiazaborinane

There total 2 articles about 1,3-dimethyl-2-dimethylaminodiazaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4375-83-1
tris(dimethylamino)borane

: 111-33-1
1,3-bis(methylamino)propane

: 3693-07-0
1,3-dimethyl-2-dimethylaminodiazaborinane

: 124-40-3
dimethyl amine

Guidance literature:: transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
DOI:10.1021/ic50086a063

Reference yield:

: 76356-55-3
1,3-dimethyl-2-(pyrazol-1'-yl)-1,3,2-diazaboracyclohexane

: 7397-47-9
(dimethylamino)diethylborane

: 3693-07-0
1,3-dimethyl-2-dimethylaminodiazaborinane

: 14695-69-3
4,4,8,8-tetraethylpyrazabole

Guidance literature:: In neat (no solvent); an equimol. amt. of Me2NBEt2 was added with stirring at 0°C under Ar to pyrazolylborane, mixt. was warmed to room temp. and heated to gentle reflux for several hours; 1,3-dimethyl-2-dimethylamino-1,3,2-diazaboracyclohexane was distilled off under reduced pressure, residual B-tetraethylpyrazabole was purified by recrystn. and characterized by spectroscopic data;
DOI:10.1016/0022-328X(83)80216-2