2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

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Chemical Name:2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester
CAS No.:75626-64-1
Molecular Formula:C₃₃H₃₅N₃O₉
Molecular Weight:617.656
Hs Code.:

Synonyms:2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

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Chemical Property of 2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

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Technology Process of 2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

There total 9 articles about 2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 75626-60-7
(Z)-methyl 4-amino-α-<<(tetrahydro-2H-pyran-2-yl)-oxy>imino>phenylacetate

: 75626-73-2
benzyl (-)-(R)-4-chloro-4-oxo-2-<<(benzyloxy)carbonyl>amino>butyrate

: 75626-64-1
2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/jo00314a029

Reference yield:

: 72531-10-3
4-<<(benzyloxy)carbonyl>amino>acetophenone

: 75626-64-1
2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 75 percent / selenium dioxide / 3 h / 100 °C

2: 59 percent / pyridine / 4 h / 0 °C

3: 98 percent / methanol; diethyl ether / 0 °C

4: 100 percent / H₂ / palladium on carbon / ethyl acetate / 0.5 h

5: 81 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

With selenium(IV) oxide; hydrogen; triethylamine; palladium on activated charcoal; In pyridine; methanol; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jo00314a029

Reference yield:

: 75626-51-6
4-<<(benzyloxy)carbonyl>amino>-α-oxophenylacetic acid

: 75626-64-1
2-Benzyloxycarbonylamino-N-(4-{methoxycarbonyl-[(Z)-tetrahydro-pyran-2-yloxyimino]-methyl}-phenyl)-succinamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / pyridine / 4 h / 0 °C

2: 98 percent / methanol; diethyl ether / 0 °C

3: 100 percent / H₂ / palladium on carbon / ethyl acetate / 0.5 h

4: 81 percent / triethylamine / CH₂Cl₂ / 0.5 h / 0 °C

With hydrogen; triethylamine; palladium on activated charcoal; In pyridine; methanol; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jo00314a029