2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol

Base Information

• Chemical Name: 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol
• CAS No.: 1453905-07-1
• Molecular Formula: C₁₆H₁₆N₂O₈
• Molecular Weight: 364.312
• Mol file: 1453905-07-1.mol

Synonyms:2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol

Chemical Property of 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol

There total 1 articles about 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-hydroxy-5-nitrobenzyl alcohol (39224-61-8) + 6-nitroveratrylbromide (53413-67-5) → 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol (1453905-07-1)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1002/chem.201301298

Reference yield: 85.0%

phosgene (75-44-5) + 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol (1453905-07-1) + 1,3-dichloro-7-hydroxy-9,9-dimethyl-9H-acridin-2(7)-one (118290-05-4) → C32H25Cl2N3O11 (1453905-13-9)

Guidance literature:

phosgene; 2-((4,5-dimethoxy-2-nitrobenzyl)oxy)-5-nitrophenylmethanol; In tetrahydrofuran; toluene; at 0 - 20 ℃; Inert atmosphere;

1,3-dichloro-7-hydroxy-9,9-dimethyl-9H-acridin-2⁽⁷⁾-one; With triethylamine; In tetrahydrofuran; toluene; at 0 ℃; for 0.25h;

DOI:10.1002/chem.201301298

upstream raw materials:

2-hydroxy-5-nitrobenzyl alcohol

6-nitroveratrylbromide

Downstream raw materials:

C₃₂H₂₅Cl₂N₃O₁₁