Technology Process of 5-O-(tert-butyldiphenylsilyl)-2-deoxy-L-ribonolactone
There total 11 articles about 5-O-(tert-butyldiphenylsilyl)-2-deoxy-L-ribonolactone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen; acetic acid;
palladium on activated charcoal;
In
methanol; acetone;
for 72h;
under 2585.7 Torr;
Ambient temperature;
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
benzene;
for 1.5h;
Heating;
DOI:10.1080/00397919408010201
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 95 percent / dimethylformamide
2: 98 percent / 10percent aq. HCl / tetrahydrofuran / 4 h / Ambient temperature
3: 86 percent / DMAP, pyridine / CH2Cl2 / 24 h / Ambient temperature
4: 79 percent / CH3I, CaCO3, water / acetonitrile; H2O / 20 h / 47 °C
5: 91 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide, 4 A sieves / CH2Cl2 / 4 h / Ambient temperature
6: 87 percent / H2, acetic acid / 10percent Pd/C / acetone; methanol / 72 h / 2585.7 Torr / Ambient temperature
With
pyridine; hydrogenchloride; dmap; tetrapropylammonium perruthennate; 4 A molecular sieve; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; calcium carbonate; methyl iodide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
