1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

Base Information

Chemical Name:1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene
CAS No.:74783-61-2
Molecular Formula:C₁₃H₁₆N₂O₆
Molecular Weight:296.28
Hs Code.:

Synonyms:1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

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Chemical Property of 1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

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Technology Process of 1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

There total 5 articles about 1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 37517-81-0
3-chloro-3-oxopropanoic acid methyl ester

: 74783-59-8
1-Amino-2-methoxy-3,4-dimethyl-6-nitrobenzene

: 74783-61-2
1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

Guidance literature:: In Petroleum ether; at 80 ℃; for 1h;

Reference yield:

: 74783-55-4
4-acetamino-1-methoxy-2,3-dimethylbenzene

: 74783-61-2
1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / conc. nitric acid / 0.17 h / -40 °C

2: conc. H₂SO₄ / 0.17 h / 80 °C

3: 75 percent / 1.) 80percent sulfuric acid, NaNO₂, 2.) 30percent hypophosphorous acid / H₂O / 144 h / Ambient temperature

4: 34 percent / NH₃ / methanol / 3 h / 200 °C / Carius tube

5: 98 percent / petroleum ether / 1 h / 80 °C

With sulfuric acid; ammonia; nitric acid; hypophosphorous acid; sodium nitrite; In methanol; water; Petroleum ether;

Reference yield:

: 74783-56-5
4-acetamino-1-methoxy-5,6-dimethyl-2,3-dinitrobenzene

: 74783-61-2
1-methoxy-2-(methoxycarbonylmethylenecarbonylamino)-5,6-dimethyl-3-nitrobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: conc. H₂SO₄ / 0.17 h / 80 °C

2: 75 percent / 1.) 80percent sulfuric acid, NaNO₂, 2.) 30percent hypophosphorous acid / H₂O / 144 h / Ambient temperature

3: 34 percent / NH₃ / methanol / 3 h / 200 °C / Carius tube

4: 98 percent / petroleum ether / 1 h / 80 °C

With sulfuric acid; ammonia; hypophosphorous acid; sodium nitrite; In methanol; water; Petroleum ether;