phenylthiodiphenylphosphine

Base Information

• Chemical Name: phenylthiodiphenylphosphine
• CAS No.: 14311-22-9
• Molecular Formula: C₁₈H₁₅PS
• Molecular Weight: 294.357

Synonyms:phenylthiodiphenylphosphine

Chemical Property of phenylthiodiphenylphosphine

Chemical Property:

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Technology Process of phenylthiodiphenylphosphine

There total 7 articles about phenylthiodiphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

thiophenol (108-98-5) + diphenylphosphane (829-85-6) → phenylthiodiphenylphosphine (14311-22-9)

Guidance literature:

[Rh(η3-benzyl)(bis(diisopropylphosphino)ethane)]; In benzene-d6; at 110 ℃; for 20h;

DOI:10.1021/ja065346+

Reference yield: 72.0%

thiophenol (108-98-5) + (diethylamino)diphenylphosphine (1636-15-3) → phenylthiodiphenylphosphine (14311-22-9)

Guidance literature:

With sodium hydride; In benzene;

Reference yield:

diphenyl trisulfide (20057-88-9) + (4-methylphenylthio)diphenylphosphan (58558-57-9) → 4-(phenyldisulfanyl)toluene (29627-34-7) + Phenyl-p-tolyl-trisulfid (16599-21-6) + Diphenyl-dithiophosphinsaere-phenylester (57644-86-7) + Diphenyl-S-p-tolyl-dithiophosphinat (102173-07-9) + phenylthiodiphenylphosphine (14311-22-9) + diphenyldisulfane (882-33-7)

Guidance literature:

In ⁽²⁾H₈-toluene; toluene; at 25 ℃; Product distribution; Mechanism; other tricoordinate phosphorous compounds;

upstream raw materials:

phenylthiotrimethylsilane

diphenyltrifluorophosphorane

diphenyl trisulfide

(4-methylphenylthio)diphenylphosphan

Downstream raw materials:

diphenylphosphine hydrogen iodide

thiophenol

iodo-diphenyl-phosphine

triphenylphosphine sulfide

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