C₃₇H₄₇N₅O₃

Base Information

Chemical Name:C₃₇H₄₇N₅O₃
CAS No.:1190769-52-8
Molecular Formula:C₃₇H₄₇N₅O₃
Molecular Weight:609.812
Hs Code.:

C<sub>37</sub>H<sub>47</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₃₇H₄₇N₅O₃

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Chemical Property of C₃₇H₄₇N₅O₃

Chemical Property:

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Technology Process of C₃₇H₄₇N₅O₃

There total 11 articles about C₃₇H₄₇N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1220106-80-8
C₄₂H₅₅N₅O₅

: 1190769-52-8
C₃₇H₄₇N₅O₃

Guidance literature:: With hydrogenchloride; methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 851544-48-4
(3aS,5R,7aS,9aS)-3-benzyl-4-oxo-decahydro-2-oxa-3,4a-diazacyclopenta[f]azulene-5-carboxylic acid tert-butyl ester

: 1190769-52-8
C₃₇H₄₇N₅O₃

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; water / 3 h / 85 °C / 7500.75 Torr

4.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Microwave irradiation

7.1: methanesulfonic acid / dichloromethane / 12 h / 20 °C / Inert atmosphere

8.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

8.2: 1 h / 20 °C / Inert atmosphere

9.1: hydrogen; citric acid / ethanol; water / 24 h / 60 °C / 45004.5 Torr

10.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

10.2: 20 °C / Inert atmosphere

11.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

12.1: hydrogenchloride; methanol / 20 °C

With hydrogenchloride; methanol; triethylsilane; sodium tetrahydroborate; methanesulfonic acid; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; citric acid; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 1151560-50-7
C₃₅H₄₅N₅O₅

: 1190769-52-8
C₃₇H₄₇N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen; citric acid / ethanol; water / 24 h / 60 °C / 45004.5 Torr

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.1: hydrogenchloride; methanol / 20 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; hydrogen; N-ethyl-N,N-diisopropylamine; citric acid; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.bmcl.2012.01.098