2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

Base Information

Chemical Name:2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide
CAS No.:886044-03-7
Molecular Formula:C₁₁H₁₃Cl₂O₂PS
Molecular Weight:311.169
Hs Code.:

Synonyms:2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

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Technology Process of 2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

There total 2 articles about 2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31758-87-9
1-(4-chlorophenyl)-2,2-dimethylpropane-1,3-diol

: 886044-03-7
2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

Guidance literature:: With trichlorophosphate; In tetrachloromethane; for 4h; Heating;
DOI:10.1080/10426500500542968 DOI:10.1080/10426500600864296

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 886044-03-7
2-chloro-4-(4-chloro-phenyl)-5,5-dimethyl-[1,3,2]dioxaphosphinane 2-sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol

2: PSCl₃ / CCl₄ / 4 h / Heating

With potassium hydroxide; trichlorophosphate; In tetrachloromethane; ethanol;
DOI:10.1080/10426500600864296