Ph₂(O)POCH₂C(pyrazolyl)3

Base Information

Chemical Name:Ph₂(O)POCH₂C(pyrazolyl)3
CAS No.:852244-11-2
Molecular Formula:C₂₃H₂₁N₆O₂P
Molecular Weight:444.433
Hs Code.:

Ph<sub>2</sub>(O)POCH<sub>2</sub>C(pyrazolyl)3

Synonyms:Ph₂(O)POCH₂C(pyrazolyl)3

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Chemical Property of Ph₂(O)POCH₂C(pyrazolyl)3

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Technology Process of Ph₂(O)POCH₂C(pyrazolyl)3

There total 1 articles about Ph₂(O)POCH₂C(pyrazolyl)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 308847-52-1
2,2,2-tris(pyrazol-1-yl)ethanol

: 1499-21-4
Diphenylphosphinic chloride

: 852244-11-2
Ph₂(O)POCH₂C(pyrazolyl)3

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 2h;
DOI:10.1039/b719023a

Reference yield: 93.0%

: 14104-20-2
silver tetrafluoroborate

: 852244-11-2
Ph₂(O)POCH₂C(pyrazolyl)3

: 1034522-25-2
[Ph₂(O)POCH₂C(pyrazolyl)3]2AgBF₄

Guidance literature:: In tetrahydrofuran; (under N2, Schlenk); AgBF4 dissolved in THF, soln. of ligand in THF added dropwise during 10 min, stirred for 3 h, hexane added, kept at -20°C for 2 h; filtered, ppt. washed with cold hexane, vac. dried; elem. anal.;
DOI:10.1039/b719023a

Reference yield: 87.0%

: 852244-11-2
Ph₂(O)POCH₂C(pyrazolyl)3

: iron(II) tetrafluoroborate hexahydrate

: [Ph₂(O)POCH₂C(pyrazolyl)3]2Fe(BF₄)2

Guidance literature:: In tetrahydrofuran; (under N2, Schlenk); Fe(BF4)2*6H2O dissolved in THF, THF soln. of ligandadded dropwise, stirred for 10 min; filtered, washed with THF, vac. dried; elem. anal.;
DOI:10.1039/b719023a