Technology Process of C39H38N6O4
There total 3 articles about C39H38N6O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2;
In
1,4-dioxane; water;
at 90 ℃;
for 14h;
Inert atmosphere;
DOI:10.1002/ejoc.201201384
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
2: bromine; disodium hydrogenphosphate / N,N-dimethyl-formamide / 6 h / 20 °C
3: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium phosphate / water; 1,4-dioxane / 14 h / 90 °C / Inert atmosphere
With
potassium phosphate; disodium hydrogenphosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; tetrabutyl ammonium fluoride; bromine;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
3: |Suzuki Coupling;
DOI:10.1002/ejoc.201201384
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bromine; disodium hydrogenphosphate / N,N-dimethyl-formamide / 6 h / 20 °C
2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium phosphate / water; 1,4-dioxane / 14 h / 90 °C / Inert atmosphere
With
potassium phosphate; disodium hydrogenphosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; bromine;
In
1,4-dioxane; water; N,N-dimethyl-formamide;
2: |Suzuki Coupling;
DOI:10.1002/ejoc.201201384
