Technology Process of C28H47BN2O8
There total 3 articles about C28H47BN2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate;
In
dimethyl sulfoxide;
at 20 - 80 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 0 - 20 °C
2.1: potassium carbonate / water; N,N-dimethyl-formamide / 20 - 45 °C
2.2: 45 °C
3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 20 - 80 °C / Inert atmosphere
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; boron tribromide; potassium carbonate;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja303304j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / water; N,N-dimethyl-formamide / 20 - 45 °C
1.2: 45 °C
2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / dimethyl sulfoxide / 20 - 80 °C / Inert atmosphere
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate; potassium carbonate;
In
water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja303304j