tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

Base Information

Chemical Name:tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate
CAS No.:1421921-04-1
Molecular Formula:C₂₇H₃₃N₃O₂S
Molecular Weight:463.644
Hs Code.:

Synonyms:tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

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Chemical Property of tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

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Technology Process of tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

There total 6 articles about tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-08-8
2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}aniline hydrobromide

: 1421922-29-3
tert-butyl N-formyl-N-methylglycinate

: 1421921-04-1
tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

Guidance literature:: tert-butyl N-formyl-N-methylglycinate; With oxalyl dichloride; In chloroform; at 20 ℃; for 0.166667h; Inert atmosphere;

2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}aniline hydrobromide; In chloroform; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: sarcosine t-butyl ester hydrochloride

: 1421921-04-1
tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / ethanol / 0.33 h / 20 °C / Cooling with ice

1.2: 1 h / 70 °C

2.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

With oxalyl dichloride; triethylamine; In ethanol; chloroform;

Reference yield:

: 1421922-04-4
2-(2,5-dimethyl-4-nitrophenyl)ethanethioamide

: 1421921-04-1
tert-butyl N-{(E)-[(2,5-dimethyl-4-{[4-(4-methylphenyl)-1,3-thiazol-2-yl]methyl}phenyl)imino]methyl}-N-methylglycinate

Guidance literature:: Multi-step reaction with 3 steps

1.1: isopropyl alcohol / 1 h / 80 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 19 h / 20 °C

3.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C / Inert atmosphere

3.2: 3 h / 20 °C / Inert atmosphere

With oxalyl dichloride; palladium 10% on activated carbon; hydrogen; In methanol; chloroform; isopropyl alcohol;