[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

Base Information

Chemical Name:[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone
CAS No.:870258-68-7
Molecular Formula:C₃₄H₃₂N₂O₄
Molecular Weight:532.639
Hs Code.:

Synonyms:[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

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Chemical Property of [(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

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Technology Process of [(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

There total 7 articles about [(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 98-88-4
benzoyl chloride

: 133603-96-0
C₂₀H₂₄N₂O₂

: 870258-68-7
[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

Guidance literature:: benzoyl chloride; C₂₀H₂₄N₂O₂; With triethylamine; In toluene; at 60 ℃;

With potassium hydroxide; In ethanol; at 20 ℃; for 6h;
DOI:10.1002/adsc.200606013

Reference yield:

: [(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-trimethylsilanyloxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

: 870258-68-7
[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

Guidance literature:: With potassium fluoride; tetrabutylammomium bromide; In water; at 20 ℃; for 2h;
DOI:10.1002/adsc.200606013

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 870258-68-7
[(2S,3S,4aR,8aR)-4-Benzoyl-2,3-bis-(2-hydroxy-phenyl)-octahydro-quinoxalin-1-yl]-phenyl-methanone

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol / 12 h / Heating

2: 52.3 g / Mn powder; CF₃COOH / acetonitrile; toluene / 24 h / 20 °C

3: Et₃N / toluene / 1 h / Heating

4: Et₃N / toluene / 0 - 20 °C

5: KF; Bu₄NBr / H₂O / 2 h / 20 °C

With potassium fluoride; manganese; tetrabutylammomium bromide; triethylamine; trifluoroacetic acid; In ethanol; water; toluene; acetonitrile;
DOI:10.1002/adsc.200606013