benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate

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Chemical Name:benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate
CAS No.:61534-94-9
Molecular Formula:C₂₃H₂₂N₂O₄S
Molecular Weight:422.505
Hs Code.:

Synonyms:benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate

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Chemical Property of benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate

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Technology Process of benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate

There total 4 articles about benzyl α-[3-phenoxymethyl-7-oxo-4-thia-2,6-diazabicyclo[3,2,0]hept-2-en-6-yl]-α-isopropenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 42879-04-9
Benzyl (1S,3S,6R)-6-(phenoxyacetylamino)penicillanate 1-oxide

: 61534-94-9,69576-06-3
4,7-diaza-7-(1-benzyloxycarbonyl-2-methylprop-2-enyl)-3-phenoxymethyl-2-thiabicyclo-<3.2.0>-hept-3-en-6-one

Guidance literature:: With phosphorous acid trimethyl ester; In benzene; for 15h; Heating;
DOI:10.1016/0040-4020(82)85002-3

Reference yield:

: 1256-06-0
(2S,5R,6R)-benzyl-3,3-dimethyl-7-oxo-6-(2-phenoxyacetamido)-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

: 61534-94-9,69576-06-3
4,7-diaza-7-(1-benzyloxycarbonyl-2-methylprop-2-enyl)-3-phenoxymethyl-2-thiabicyclo-<3.2.0>-hept-3-en-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 degC, 30 min, 10 degC, 30 min

2: 72 percent / trimethyl phosphite / benzene / 15 h / Heating

With 3-chloro-benzenecarboperoxoic acid; phosphorous acid trimethyl ester; In dichloromethane; benzene;
DOI:10.1016/0040-4020(82)85002-3

Reference yield:

: 100-39-0
benzyl bromide

: 61534-94-9,69576-06-3
4,7-diaza-7-(1-benzyloxycarbonyl-2-methylprop-2-enyl)-3-phenoxymethyl-2-thiabicyclo-<3.2.0>-hept-3-en-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / dimethylformamide / 24 h / Ambient temperature

2: 85 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 degC, 30 min, 10 degC, 30 min

3: 72 percent / trimethyl phosphite / benzene / 15 h / Heating

With 3-chloro-benzenecarboperoxoic acid; phosphorous acid trimethyl ester; In dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/0040-4020(82)85002-3