(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

Base Information

Chemical Name:(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine
CAS No.:1472104-58-7
Molecular Formula:C₁₄H₂₂N₂O₂
Molecular Weight:250.341
Hs Code.:

Synonyms:(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

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Chemical Property of (2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

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Technology Process of (2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

There total 4 articles about (2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66684-61-5
1,5-difluoro-3-methoxy-2-nitrobenzene

: 1472104-58-7
(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide; water / dimethyl sulfoxide / 21 h / 23 - 60 °C

2: dimethyl sulfoxide / 2 h / 23 - 100 °C

3: caesium carbonate / dichloromethane; acetonitrile / 2 h / 23 °C

4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 16.33 h / 120 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / methanol / 16.33 h / 2585.81 Torr / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; palladium 10% on activated carbon; water; hydrogen; caesium carbonate; sodium hydroxide; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1472104-55-4
3-methoxy-5-morpholin-4-yl-2-nitrophenol

: 1472104-58-7
(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / dichloromethane; acetonitrile / 2 h / 23 °C

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 16.33 h / 120 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 16.33 h / 2585.81 Torr / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; palladium 10% on activated carbon; hydrogen; caesium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1472104-56-5
trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

: 1472104-58-7
(2-isopropyl-6-methoxy-4-morpholin-4-yl-phenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / N,N-dimethyl-formamide / 16.33 h / 120 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 16.33 h / 2585.81 Torr / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; palladium 10% on activated carbon; hydrogen; In methanol; N,N-dimethyl-formamide;