trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

Base Information

Chemical Name:trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester
CAS No.:1472104-56-5
Molecular Formula:C₁₂H₁₃F₃N₂O₇S
Molecular Weight:386.306
Hs Code.:

Synonyms:trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

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Chemical Property of trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

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Technology Process of trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

There total 3 articles about trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 1472104-55-4
3-methoxy-5-morpholin-4-yl-2-nitrophenol

: 1472104-56-5
trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

Guidance literature:: With caesium carbonate; In dichloromethane; acetonitrile; at 23 ℃; for 2h;

Reference yield:

: 66684-61-5
1,5-difluoro-3-methoxy-2-nitrobenzene

: 1472104-56-5
trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; water / dimethyl sulfoxide / 21 h / 23 - 60 °C

2: dimethyl sulfoxide / 2 h / 23 - 100 °C

3: caesium carbonate / dichloromethane; acetonitrile / 2 h / 23 °C

With water; caesium carbonate; sodium hydroxide; In dichloromethane; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 256454-00-9
5-fluoro-3-methoxy-2-nitrophenol

: 1472104-56-5
trifluoromethanesulfonic acid (3-methoxy-5-morpholin-4-yl-2-nitrophenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 2 h / 23 - 100 °C

2: caesium carbonate / dichloromethane; acetonitrile / 2 h / 23 °C

With caesium carbonate; In dichloromethane; dimethyl sulfoxide; acetonitrile;