(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

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Chemical Name:(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one
CAS No.:1430324-79-0
Molecular Formula:C₂₅H₂₈N₆O₇
Molecular Weight:524.533
Hs Code.:

Synonyms:(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

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Chemical Property of (5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

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Technology Process of (5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

There total 8 articles about (5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1430324-78-9
4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]aniline

: 1112978-29-6
(5Z) 5-(1,3-benzodioxol-5-yl)methylene-2-ethylthio-3,5-dihydro-4H-imidazol-4-one

: 1430324-79-0
(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

Guidance literature:: In hexane; Sealed tube; Microwave irradiation;
DOI:10.1016/j.ejmech.2013.01.035

Reference yield:

: 54840-15-2
4-N-tert-butoxycarbonylaminophenol

: 1430324-79-0
(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / tetrahydrofuran / 48 h / 80 °C

2: triethylamine / dichloromethane / 24.33 h / 0 - 25 °C

3: sodium azide / water; ethanol / 1 h / 160 °C / Sealed tube; Microwave irradiation

4: hexane / 30?min / 160?°C / Sealed tube; Microwave irradiation

With sodium azide; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1016/j.ejmech.2013.01.035

Reference yield:

: 77544-60-6
p-toluenesulfonic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester

: 1430324-79-0
(5Z)-2-[4-[2-[2-[2-(2-azidoethoxy)ethoxy]ethoxy]ethoxy]phenylamino]-5-(benzo[1,3]dioxol-5-ylmethylene)-3,5-dihydroimidazol-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / tetrahydrofuran / 48 h / 80 °C

2: triethylamine / dichloromethane / 24.33 h / 0 - 25 °C

3: sodium azide / water; ethanol / 1 h / 160 °C / Sealed tube; Microwave irradiation

4: hexane / 30?min / 160?°C / Sealed tube; Microwave irradiation

With sodium azide; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water;
DOI:10.1016/j.ejmech.2013.01.035