(+)-muscarine toluene-p-sulfonate salt

Base Information

Chemical Name:(+)-muscarine toluene-p-sulfonate salt
CAS No.:82083-43-0
Molecular Formula:C₇H₇O₃S*C₉H₂₀NO₂
Molecular Weight:345.46
Hs Code.:

Synonyms:(+)-muscarine toluene-p-sulfonate salt

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Chemical Property of (+)-muscarine toluene-p-sulfonate salt

Chemical Property:

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Technology Process of (+)-muscarine toluene-p-sulfonate salt

There total 26 articles about (+)-muscarine toluene-p-sulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75499-91-1,112020-34-5
2,5-anhydro-1,4-dideoxy-6-O-(p-tolylsulphonyl)-D-ribo-hexitol

: 75-50-3
trimethylamine

: 82083-43-0
(+)-muscarine toluene-p-sulfonate salt

Guidance literature:: In methanol;

Reference yield:

: 6014-42-2
L-rhamnose

: 82083-43-0
(+)-muscarine toluene-p-sulfonate salt

Guidance literature:: Multi-step reaction with 7 steps

1: 1) BaCO₃, Br₂, 2) CF₃CO₂H / 1) H₂O, a) 0 deg C, 1 h, b) r.t., 6 h, 2) H₂O, r.t., 4 h

2: 58 percent / pyridine, 4-(N,N-dimethylamino)pyridine / 7 h / Ambient temperature

3: 79 percent / trifluoroacetic anhydride, Et₃N / tetrahydrofuran / a) -78 deg C, 30 min, b) -25 deg C, 30 min

4: 76 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h

5: 1) LiBH₄, 2) NaOAc / 1) THF, 0 deg C to r.t., 15 min, 2) MeCN, reflux, 8 h

6: 77 percent / pyridine / 16 h / Ambient temperature

7: 67 percent / methanol / 6 h / 80 °C

With pyridine; dmap; lithium borohydride; hydrogen; bromine; sodium acetate; triethylamine; barium carbonate; trifluoroacetic acid; trifluoroacetic anhydride; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1039/P19920003023

Reference yield:

: 138480-29-2
2-O-methanesulfonyl-3,6-dideoxy-L-erythro-hex-2-enono-1,4-lactone

: 82083-43-0
(+)-muscarine toluene-p-sulfonate salt

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h

2: 1) LiBH₄, 2) NaOAc / 1) THF, 0 deg C to r.t., 15 min, 2) MeCN, reflux, 8 h

3: 77 percent / pyridine / 16 h / Ambient temperature

4: 67 percent / methanol / 6 h / 80 °C

With pyridine; lithium borohydride; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1039/P19920003023