RuCl(C₃₂H₁₆N₈)*C₈H₄N₂

Base Information

• Chemical Name: RuCl(C₃₂H₁₆N₈)*C₈H₄N₂
• CAS No.: 14096-15-2
• Molecular Formula: C₄₀H₂₀ClN₁₀Ru
• Molecular Weight: 777.189
• Mol file: 14096-15-2.mol

Synonyms:RuCl(C₃₂H₁₆N₈)*C₈H₄N₂

Chemical Property of RuCl(C₃₂H₁₆N₈)*C₈H₄N₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of RuCl(C₃₂H₁₆N₈)*C₈H₄N₂

There total 1 articles about RuCl(C₃₂H₁₆N₈)*C₈H₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ruthenium(III) chloride trihydrate (14898-67-0) + phthalonitrile (91-15-6) → RuCl(C32H16N8)*C8H4N2 (14096-15-2)

Guidance literature:

In neat (no solvent); triturating RuCl3*3H2O with an excess of 1.2-dicyanobenzene under N2; heating at 290 °C for 2-3 h;; extraction with acetone in a Soxhlet app.;;

DOI:10.1016/0022-1902(65)80095-1

Reference yield:

RuCl(C32H16N8)*C8H4N2 (14096-15-2) → Ru(3+)*Cl(1-)*C32H16N8(2-)={RuCl(C32H16N8)} (47829-08-3) + phthalonitrile (91-15-6)

Guidance literature:

In neat (no solvent); removal of 1.2-dicyanobenzene on heating at 500 °C;;

Reference yield:

RuCl(C32H16N8)*C8H4N2 (14096-15-2) + aniline (62-53-3) → {Ru(C32H16N8)(C6H5NH2)2}*4C6H5NH2

Guidance literature:

In neat (no solvent); extraction with boiling aniline;;

DOI:10.1016/0022-1902(65)80095-1

upstream raw materials:

ruthenium(III) chloride trihydrate

phthalonitrile

Downstream raw materials:

Ru⁽³⁺⁾*Cl^(1-)*C₃₂H₁₆N₈^(2-)={RuCl(C₃₂H₁₆N₈)}

phthalonitrile