methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose

Base Information

• Chemical Name: methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose
• CAS No.: 149405-18-5
• Molecular Formula: C₁₉H₂₄O₅S₂
• Molecular Weight: 396.529
• Mol file: 149405-18-5.mol

Synonyms:methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose

Chemical Property of methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose

Chemical Property:

Purity/Quality:

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Technology Process of methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose

There total 1 articles about methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

carbon disulfide (75-15-0,12122-00-8) + methyl 4,6-O-(phenylmethylene)-3-deoxy-α-D-erythro-hexopyranoside-2-ulose (74524-02-0) + ethyl iodide (75-03-6) → methyl 4,6-O-benzylidene-3--3-deoxy-α-D-erythro-hexopyranosid-2-ulose (149405-18-5)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; paraffin; benzene; at 20 ℃; for 1h;

DOI:10.1016/0008-6215(92)84041-P

upstream raw materials:

carbon disulfide

methyl 4,6-O-(phenylmethylene)-3-deoxy-α-D-erythro-hexopyranoside-2-ulose

ethyl iodide