1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Base Information

Chemical Name:1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane
CAS No.:94650-69-8
Molecular Formula:C₂₈H₄₆O₉
Molecular Weight:526.668
Hs Code.:

1,14-Bis<tetrahydropyran-2-yloxy>-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Synonyms:1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

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Chemical Property of 1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Chemical Property:

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Technology Process of 1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

There total 4 articles about 1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5631-96-9
2-(2-chloroethoxy)-tetrahydro-2H-pyrane

: 80525-60-6,118917-64-9
4-Benzyloxymethyl-3,6-dioxa-1,8-octanediol

: 94650-69-8
1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; at 65 ℃; for 72h;
DOI:10.1021/jo00265a026

Reference yield:

: 54533-84-5
2-(2-(2-chloroethoxy)ethoxy)tetrahydro-2H-pyran

: 13071-59-5,17325-85-8,56552-80-8,4799-67-1
3-benzyloxypropan-1,2-diol

: 94650-69-8
1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; at 65 ℃; for 72h;
DOI:10.1021/jo00265a026

Reference yield:

: 13071-59-5,17325-85-8,56552-80-8,4799-67-1
3-benzyloxypropan-1,2-diol

: 94650-69-8
1,14-Bis-7-benzyloxymethyl-3,6,9,12-tetraoxatetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: 50percent aq. sodium hydroxide / tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

2: aq. HCl / methanol; CH₂Cl₂ / 2 h / Ambient temperature

3: 50percent aq. sodium hydroxide / tetrabutylammonium hydrogen sulfate / 72 h / 65 °C

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane;
DOI:10.1021/jo00265a026