3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Base Information

Chemical Name:3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical
CAS No.:124558-40-3
Molecular Formula:C₂₄H₂₈NO₂S
Molecular Weight:394.558
Hs Code.:

Synonyms:3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

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Chemical Property of 3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

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Technology Process of 3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

There total 3 articles about 3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 83078-71-1
C₁₇H₂₀NO₂

: 100-53-8
phenylmethanethiol

: 124558-40-3
3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 16h;
DOI:10.1055/s-1989-27306

Reference yield:

: 71051-83-7
3-formyl-2,2,5,5-tetramethyl-pyrroline-1-oxyl

: 124558-40-3
3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 10percent aq. NaOH / ethanol / 3 h / 25 °C

2: 90 percent / TBAF / tetrahydrofuran / 16 h / 25 °C

With sodium hydroxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol;
DOI:10.1055/s-1989-27306

Reference yield:

: 98-86-2
acetophenone

: 124558-40-3
3-(1-Benzylthio-3-oxo-3-phenylpropyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 10percent aq. NaOH / ethanol / 3 h / 25 °C

2: 90 percent / TBAF / tetrahydrofuran / 16 h / 25 °C

With sodium hydroxide; tetrabutyl ammonium fluoride; In tetrahydrofuran; ethanol;
DOI:10.1055/s-1989-27306