Technology Process of C66H63N7O9
There total 7 articles about C66H63N7O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 79 percent / DEAD; TPP / tetrahydrofuran / Heating
2.1: 77 percent / MCPBA / CH2Cl2 / 20 °C
3.1: (Ac)2O / Heating
3.2: 81 percent / NaOH / H2O / Heating
4.1: 62 percent / DMSO; Py-SO3; Et3N / 20 °C
5.1: 77 percent / NaClO2; H2NSO3 / acetone; H2O / 20 °C
6.1: 67 percent / DCCI / dimethylformamide / 20 °C
7.1: 83 percent / dimethylformamide / 48 h / 20 °C
With
sodium chlorite; aminosulfonic acid; sulfur trioxide pyridine complex; acetic anhydride; thiamine diphosphate; dimethyl sulfoxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; diethylazodicarboxylate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tetlet.2004.12.115
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 77 percent / NaClO2; H2NSO3 / acetone; H2O / 20 °C
2: 67 percent / DCCI / dimethylformamide / 20 °C
3: 83 percent / dimethylformamide / 48 h / 20 °C
With
sodium chlorite; aminosulfonic acid; dicyclohexyl-carbodiimide;
In
water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tetlet.2004.12.115