diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

Base Information

Chemical Name:diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate
CAS No.:699000-89-0
Molecular Formula:C₁₈H₂₉ClNO₄P
Molecular Weight:389.859
Hs Code.:

Synonyms:diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

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Technology Process of diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

There total 3 articles about diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 699000-76-5
diethyl {[(E)-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

: 699000-89-0
diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

Guidance literature:: With N-chloro-succinimide; In tetrachloromethane; for 1h; Heating;
DOI:10.1055/s-2004-815969

Reference yield:

: 110470-34-3,110548-53-3,110548-54-4,112564-56-4
diethyl [1-amine(4-methoxyphenyl)methyl]phosphonate

: 699000-89-0
diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / MgSO₄ / CH₂Cl₂ / 3 h / Heating

2: 99 percent / N-chlorosuccinimide / CCl₄ / 1 h / Heating

With N-chloro-succinimide; magnesium sulfate; In tetrachloromethane; dichloromethane;
DOI:10.1055/s-2004-815969

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 699000-89-0
diethyl {[(E)-2-chloro-2-ethyl-1-butylidene]amino}(4-methoxyphenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / NH₄OAc; LiClO₄; 4 Angstroem molecular sieves / ethanol / 120 h / Heating

2: 98 percent / MgSO₄ / CH₂Cl₂ / 3 h / Heating

3: 99 percent / N-chlorosuccinimide / CCl₄ / 1 h / Heating

With N-chloro-succinimide; 4 A molecular sieve; ammonium acetate; lithium perchlorate; magnesium sulfate; In tetrachloromethane; ethanol; dichloromethane;
DOI:10.1055/s-2004-815969