1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene

Base Information

• Chemical Name: 1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene
• CAS No.: 102688-77-7
• Molecular Formula: C₁₄H₁₃ClO₂S₂
• Molecular Weight: 312.841
• Mol file: 102688-77-7.mol

Synonyms:1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene

Chemical Property of 1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene

There total 1 articles about 1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dimethyldisulphide (624-92-0) + 1-chloro-4-((phenylsulfonyl)methyl)benzene (51229-56-2) → 1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene (102688-77-7)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) DMSO, r.t., 20 min, 2.) 40 min;

DOI:10.1055/s-1985-31888

Reference yield: 72.0%

1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene (102688-77-7) → 4-chlorobenzaldehyde (104-88-1)

Guidance literature:

at 150 ℃; under 1 Torr;

DOI:10.1055/s-1986-31840

Reference yield:

1-(Benzenesulfonyl-methylsulfanyl-methyl)-4-chloro-benzene (102688-77-7) → C14H12(2)HClO2S2 (109635-33-8)

Guidance literature:

With water-d2; sodium hydride; Yield given. Multistep reaction; 1.) THF, 30 min, r.t., 2.) 20 min, r.t.;

DOI:10.1055/s-1986-31840

upstream raw materials:

Dimethyldisulphide

1-chloro-4-((phenylsulfonyl)methyl)benzene

Downstream raw materials:

4-chlorobenzaldehyde

C₁₄H₁₂⁽²⁾HClO₂S₂

p-chlorobenzaldehyde-d1