dibenzoyl-fumaric acid diethyl ester

Base Information

Chemical Name:dibenzoyl-fumaric acid diethyl ester
CAS No.:59726-54-4
Molecular Formula:C₂₂H₂₀O₆
Molecular Weight:380.397
Hs Code.:

Synonyms:dibenzoyl-fumaric acid diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzoyl-fumaric acid diethyl ester

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Technology Process of dibenzoyl-fumaric acid diethyl ester

There total 7 articles about dibenzoyl-fumaric acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 59726-54-4,60903-90-4
diethyl 2,3-dibenzoylbut-2-enedioate

Guidance literature:: With N-Bromosuccinimide; potassium tert-butylate; In tetrahydrofuran; at 20 ℃;
DOI:10.1080/00397910701578123

Reference yield: 46.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 60474-27-3
ethyl 5-phenyl-1,2,3-thiadiazole-4-carboxylate

: 170656-69-6
1,1'-bis(diphenylthiophosphoryl)ferrocene

: 59726-54-4,60903-90-4
diethyl 2,3-dibenzoylbut-2-enedioate

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; In chlorobenzene; at 130 ℃; for 6h; Sealed tube; Inert atmosphere;
DOI:10.1039/d1ob00116g

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 60903-90-4
diethyl 2,3-dibenzoylmaleate

: 59726-54-4
dibenzoyl-fumaric acid diethyl ester

Guidance literature:: With [bis(acetoxy)iodo]benzene; magnesium oxide; copper(II) bis(trifluoromethanesulfonate); In dimethyl sulfoxide; at 100 ℃; for 0.0833333h; Reagent/catalyst; Overall yield = 42%; Overall yield = 0.78 g; Microwave irradiation;
DOI:10.1021/acs.orglett.7b03413