2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE

Base Information

Chemical Name:2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE
CAS No.:77942-13-3
Molecular Formula:C12H16 O3
Molecular Weight:208.257
Hs Code.:2914509090
Mol file:77942-13-3.mol

Synonyms:2’’,4’’-DIMETHOXY-3’’-METHYLPROPIOPHENONE

Suppliers and Price of 2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
1-(2,4-DIMETHOXY-3-METHYL-PHENYL)-PROPAN-1-ONE Aldrich
1ea
$ 57.00

Total 2 raw suppliers

Chemical Property of 2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE

Chemical Property:

Vapor Pressure:0.000216mmHg at 25°C
Melting Point:40–41°C
Refractive Index:1.497
Boiling Point:326.4°C at 760 mmHg
Flash Point:142.3°C
PSA：35.53000
Density:1.032g/cm³
LogP:2.60490

Purity/Quality:: 1-(2,4-DIMETHOXY-3-METHYL-PHENYL)-PROPAN-1-ONE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE

There total 3 articles about 2'',4''-DIMETHOXY-3''-METHYLPROPIOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5673-07-4
2,6-dimethoxytoluene

: 79-03-8
propionyl chloride

: 77942-13-3
2',4'-dimethoxy-3'-methylpropiophenone

Guidance literature:: With titanium tetrachloride; In benzene; at 0 ℃; for 0.5h;
DOI:10.1002/1521-3773(20010903)40:17<3186::AID-ANIE3186>3.0.CO;2-W

Reference yield: 86.0%

: 63876-46-0
1-(2,4-dihydroxy-3-methylphenyl)propan-1-one

: 77-78-1
dimethyl sulfate

: 77942-13-3
2',4'-dimethoxy-3'-methylpropiophenone

Guidance literature:: With potassium carbonate; In acetone; for 48h; Heating;
DOI:10.1039/P19810000471

Reference yield:

: 608-25-3
2-methylbenzene-1,3-diol

: 77942-13-3
2',4'-dimethoxy-3'-methylpropiophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / boron trifluoride etherate / 6 h / 75 °C

2: 86 percent / potassium carbonate / acetone / 48 h / Heating

With boron trifluoride diethyl etherate; potassium carbonate; In acetone;
DOI:10.1039/P19810000471