(Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide

Base Information

Chemical Name:(Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide
CAS No.:143539-91-7
Molecular Formula:C₁₈H₂₅NO₅
Molecular Weight:335.4
Hs Code.:

Synonyms:(Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide

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Technology Process of (Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide

There total 1 articles about (Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 622-30-0
N-benzyl hydroxylalmine

: 13039-93-5
2,2:4,5-di-O-isopropylidene-D-arabinose

: 143539-91-7
(Z)-N-(1-deoxy-2,3:4,5-di-O-isopropylidene-D-mannito-1-ylidene)benzylamine N-oxide

Guidance literature:: With sodium sulfate; In dichloromethane; for 10h; Ambient temperature;
DOI:10.1016/S0040-4039(00)74694-6

Reference yield: 89.0%

: 13169-00-1
Methoxyallene

: 1104460-72-1,143539-91-7
C₁₈H₂₅NO₅

: 851959-99-4
(3R,4'S,5'R,4''R)-2-benzyl-3-(2',2',2'',2''-tetramethyl-[4',4'']bi[[1,3]dioxolanyl]-5'-yl)-4-methoxy-3,6-dihydro-2H-1,2-oxazine

Guidance literature:: Methoxyallene; With n-butyllithium; In diethyl ether; hexane; at -40 ℃; for 0.25h; Inert atmosphere;

C₁₈H₂₅NO₅; With diethylaluminium chloride; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol802514m

Reference yield: 79.0%

: 1104460-72-1,143539-91-7
C₁₈H₂₅NO₅

: 67515-49-5
1-benzyloxyallene

: 1104460-74-3
(3S,4'S,4''R,5'R)-2-benzyl-4-(benzyloxy)-3-(2',2',2'',2''-tetramethyl-4',4''-bi-1,3-dioxolan-5'-yl)-3,6-dihydro-2H-1,2-oxazine

Guidance literature:: 1-benzyloxyallene; With n-butyllithium; In diethyl ether; hexane; at -40 ℃; for 0.25h; Inert atmosphere;

C₁₈H₂₅NO₅; With diethylaluminium chloride; In diethyl ether; hexane; at -78 - 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol802514m