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1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Base Information Edit
  • Chemical Name:1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine
  • CAS No.:960595-41-9
  • Molecular Formula:C16H25NSi
  • Molecular Weight:259.467
  • Hs Code.:
  • Mol file:960595-41-9.mol
1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine

Synonyms:1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine

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Chemical Property of 1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine Edit
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Technology Process of 1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine

There total 1 articles about 1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
2-(2-methylphenyl)propanenitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
tert-butyldimethylsilyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403342
Guidance literature:
1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine; benzaldehyde; With tetrachlorosilane; chiral bisphosphoramide catalyst; In dichloromethane; at -78 ℃; for 2h;
With potassium fluoride; sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 3h; Further stages. Title compound not separated from byproducts.;
DOI:10.1021/ja077134y
Guidance literature:
benzaldehyde; With tetrachlorosilane; Denmark's dimeric catalyst; In dichloromethane; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
1-(1,1-dimethylethyl)-N-[2-(2-methylphenyl)-1-propenylidene]-1,1-dimethylsilanamine; In dichloromethane; at -78 ℃; for 2.08333h; Overall yield = 74 %; Overall yield = 187 mg; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201403342
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