(3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

Base Information

Chemical Name:(3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone
CAS No.:122969-21-5
Molecular Formula:C₂₄H₃₇NO₂
Molecular Weight:371.563
Hs Code.:

Synonyms:(3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

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Chemical Property of (3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

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Technology Process of (3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

There total 2 articles about (3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872-50-4,26138-58-9
1-methyl-pyrrolidin-2-one

: 122968-43-8
(E)-1-(2,4,6-triisopropylphenyl)-2-buten-1-one

: 122969-21-5
(3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

: 122969-22-6
(R)-1-Methyl-3-[(S)-1-methyl-3-oxo-3-(2,4,6-triisopropyl-phenyl)-propyl]-pyrrolidin-2-one

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 4h; Yield given. Yields of byproduct given;
DOI:10.1021/jo00288a027

Reference yield:

: 717-74-8
1,3,5-triisopropyl benzene

: 122969-21-5
(3RS,1'RS)-1-methyl-3-(1'-methyl-3'-oxo-3'-(2,4,6-triisopropylphenyl)propyl)-2-pyrrolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / AlCl₃ / CS₂ / Heating

2: LDA / tetrahydrofuran / 4 h / -78 °C

With aluminium trichloride; lithium diisopropyl amide; In tetrahydrofuran; carbon disulfide;
DOI:10.1021/jo00288a027