C₂₉H₂₇ClN₆O₄

Base Information

Chemical Name:C₂₉H₂₇ClN₆O₄
CAS No.:1316761-69-9
Molecular Formula:C₂₉H₂₇ClN₆O₄
Molecular Weight:559.024
Hs Code.:

C<sub>29</sub>H<sub>27</sub>ClN<sub>6</sub>O<sub>4</sub>

Synonyms:C₂₉H₂₇ClN₆O₄

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Chemical Property of C₂₉H₂₇ClN₆O₄

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Technology Process of C₂₉H₂₇ClN₆O₄

There total 9 articles about C₂₉H₂₇ClN₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1316761-71-3
ethyl 6-(2-(bis(4-methoxybenzyl)amino)pyrimidin-5-yl)-4-oxo-4,5-dihydropyrazolo[1,5-a]pyrazine-2-carboxylate

: 1316761-69-9
C₂₉H₂₇ClN₆O₄

Guidance literature:: C₂₉H₂₈N₆O₅; With N,N-dimethyl-aniline; trichlorophosphate; at 80 - 90 ℃; for 45h;

With sodium hydrogencarbonate; pH=~ 8; Cooling with ice;

Reference yield:

: 854391-95-0
bis(4-methoxybenzyl)amine hydrochloride

: 1316761-69-9
C₂₉H₂₇ClN₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 1 h / 160 °C

2.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 22 h / 100 °C

2.2: 1 h

3.1: triethylamine; trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran / 2 h / 0 °C

3.2: 1 h / 0 °C

4.1: potassium carbonate / acetone / 20 °C

5.1: ammonium acetate / ethanol / 1 h / 150 °C / Microwave irradiation

6.1: trichlorophosphate; N,N-dimethyl-aniline / 45 h / 80 - 90 °C

6.2: pH ~ 8 / Cooling with ice

With trimethylsilyl trifluoromethanesulfonate; ammonium acetate; potassium carbonate; N,N-dimethyl-aniline; triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1272403-00-5
5-bromo-N,N-bis[(4-methoxyphenyl)methyl]pyrimidin-2-amine

: 1316761-69-9
C₂₉H₂₇ClN₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 22 h / 100 °C

1.2: 1 h

2.1: triethylamine; trimethylsilyl trifluoromethanesulfonate / tetrahydrofuran / 2 h / 0 °C

2.2: 1 h / 0 °C

3.1: potassium carbonate / acetone / 20 °C

4.1: ammonium acetate / ethanol / 1 h / 150 °C / Microwave irradiation

5.1: trichlorophosphate; N,N-dimethyl-aniline / 45 h / 80 - 90 °C

5.2: pH ~ 8 / Cooling with ice

With trimethylsilyl trifluoromethanesulfonate; ammonium acetate; potassium carbonate; N,N-dimethyl-aniline; triethylamine; trichlorophosphate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetone;