Technology Process of C18H22O3
There total 2 articles about C18H22O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: oxygen; palladium diacetate / dimethyl sulfoxide / Inert atmosphere
2: pyridinium p-toluenesulfonate / toluene / 12 h / 10 - 24 °C / Inert atmosphere
With
oxygen; palladium diacetate; pyridinium p-toluenesulfonate;
In
dimethyl sulfoxide; toluene;
DOI:10.1021/ja307497h
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanesulfonamide / tetrahydrofuran; tert-butyl alcohol / Inert atmosphere
2: oxygen; palladium diacetate / dimethyl sulfoxide / Inert atmosphere
3: pyridinium p-toluenesulfonate / toluene / 12 h / 10 - 24 °C / Inert atmosphere
With
methanesulfonamide; oxygen; palladium diacetate; pyridinium p-toluenesulfonate;
In
tetrahydrofuran; dimethyl sulfoxide; toluene; tert-butyl alcohol;
DOI:10.1021/ja307497h
- Guidance literature:
-
C18H22O3; (trimethylsilyl)methylmagnesium chloride;
With
copper(l) iodide;
In
tetrahydrofuran; diethyl ether;
at -50 - 24 ℃;
for 0.5h;
Inert atmosphere;
chloro-trimethyl-silane;
With
N,N,N,N,N,N-hexamethylphosphoric triamide; triethylamine;
In
tetrahydrofuran; diethyl ether;
at -78 - 24 ℃;
for 1.5h;
Inert atmosphere;
With
palladium diacetate;
In
acetonitrile;
at 24 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja307497h
