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4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal

Base Information Edit
  • Chemical Name:4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal
  • CAS No.:85393-98-2
  • Molecular Formula:C33H42O5
  • Molecular Weight:518.693
  • Hs Code.:
  • Mol file:85393-98-2.mol
4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal

Synonyms:4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal

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Chemical Property of 4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal Edit
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Technology Process of 4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal

There total 1 articles about 4-(3'β-benzyloxy-17'β-hydroxy-5'β-androst-15'-en-17'α-yl)furan-2-carbaldehyde ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 10 steps
1: 4-dimethylaminopyridine / pyridine / 72 h / Ambient temperature
2: CaCO3 / acetone; H2O / 96 h / Heating
3: H2 / 10percent Pd/CaCO3 / ethanol / Ambient temperature
4: 1N HCl / tetrahydrofuran / 1 h
5: NaBH4 / tetrahydrofuran; methanol / Ambient temperature
6: 85 percent / m-chloroperbenzoic acid, NaOAc / CH2Cl2 / 2 h / in an ice-bath
7: 73 percent / NaOAc / benzene / 1 h / Heating
8: 90 percent / SOCl2 / pyridine / 1 h / in an ice-bath
9: 1N KOH / tetrahydrofuran; methanol / 1 h / Ambient temperature
10: CrO3/dipyridine / CH2Cl2 / 0.17 h / Ambient temperature
With chromium(VI) oxide; hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; dipyridine; hydrogen; sodium acetate; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; dmap; Lindlar's catalyst; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; acetone; benzene;
DOI:10.1002/hlca.19820650712
Guidance literature:
Multi-step reaction with 9 steps
1: 4-dimethylaminopyridine / pyridine / 72 h / Ambient temperature
2: CaCO3 / acetone; H2O / 96 h / Heating
3: H2 / 10percent Pd/CaCO3 / ethanol / Ambient temperature
4: 1N HCl / tetrahydrofuran / 1 h
5: NaBH4 / tetrahydrofuran; methanol / Ambient temperature
6: 85 percent / m-chloroperbenzoic acid, NaOAc / CH2Cl2 / 2 h / in an ice-bath
7: 73 percent / NaOAc / benzene / 1 h / Heating
8: 90 percent / SOCl2 / pyridine / 1 h / in an ice-bath
9: 1N KOH / tetrahydrofuran; methanol / 1 h / Ambient temperature
With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; hydrogen; sodium acetate; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; dmap; Lindlar's catalyst; In tetrahydrofuran; pyridine; methanol; ethanol; dichloromethane; water; acetone; benzene;
DOI:10.1002/hlca.19820650712
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