Technology Process of C23H21FO6
There total 5 articles about C23H21FO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H23FO6;
With
sodium hydroxide;
In
tetrahydrofuran; methanol; water;
for 1.5h;
Reflux;
With
hydrogenchloride;
In
methanol; water;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 2 h / 20 °C / Cooling with ice
1.2: 20 °C
2.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 6 h / 50 °C
3.1: sodium hydroxide / water; tetrahydrofuran; methanol / 1.5 h / Reflux
3.2: 20 °C
With
boron tribromide; potassium carbonate; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hexamethylenetetramine / 2.5 h / 80 °C
2.1: SULFAMIDE; sodium chlorite / 1,4-dioxane; water / 0.5 h / Cooling with ice
3.1: boron tribromide / dichloromethane / 2 h / 20 °C / Cooling with ice
3.2: 20 °C
4.1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 6 h / 50 °C
5.1: sodium hydroxide / water; tetrahydrofuran; methanol / 1.5 h / Reflux
5.2: 20 °C
With
sodium chlorite; hexamethylenetetramine; boron tribromide; potassium carbonate; SULFAMIDE; sodium iodide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;