C₁₅H₁₅Cl₂NO₃

Base Information

Chemical Name:C₁₅H₁₅Cl₂NO₃
CAS No.:1268246-30-5
Molecular Formula:C₁₅H₁₅Cl₂NO₃
Molecular Weight:328.195
Hs Code.:

C<sub>15</sub>H<sub>15</sub>Cl<sub>2</sub>NO<sub>3</sub>

Synonyms:C₁₅H₁₅Cl₂NO₃

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Chemical Property of C₁₅H₁₅Cl₂NO₃

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Technology Process of C₁₅H₁₅Cl₂NO₃

There total 5 articles about C₁₅H₁₅Cl₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-24-7
acetic anhydride

: 278597-30-1
[3-(2,6-dichlorophenyl)-5-(propan-2-yl)-1,2-oxazol-4-yl]methanol

: 1268246-30-5
C₁₅H₁₅Cl₂NO₃

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 1268246-30-5
C₁₅H₁₅Cl₂NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 24 h / 90 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 16 h / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.2: 0.17 h / 0 °C

5.1: triethylamine / dichloromethane / 20 °C

With N-chloro-succinimide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium methylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 25185-95-9
2,6-dichlorobenzaldoxime

: 1268246-30-5
C₁₅H₁₅Cl₂NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 20 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 16 h / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

3.2: 0.17 h / 0 °C

4.1: triethylamine / dichloromethane / 20 °C

With N-chloro-succinimide; lithium aluminium tetrahydride; sodium methylate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;