Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

Base Information

Chemical Name:Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester
CAS No.:162792-24-7
Molecular Formula:C₄₇H₅₆NO₆P
Molecular Weight:761.938
Hs Code.:

Synonyms:Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

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Chemical Property of Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

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Technology Process of Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

There total 14 articles about Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 162792-23-6
1D-2,4,5,6-tetra-O-benzyl-3-deoxy-myo-inositol

: 162792-24-7
Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

Guidance literature:: With N,N-diisopropylamine tetrazolide; In dichloromethane; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(97)10003-5

Reference yield:

: 162792-21-4
(1R,2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-methoxymethoxy-cyclohexanol

: 162792-24-7
Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NaH, Bu₄NI / dimethylformamide / Ambient temperature

2: 77 percent / conc. HCl / methanol / 2 h / Heating

3: 100 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 24 h / Ambient temperature

With hydrogenchloride; N,N-diisopropylamine tetrazolide; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(97)10003-5

Reference yield:

: 162792-22-5
C₃₆H₄₀O₆

: 162792-24-7
Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / conc. HCl / methanol / 2 h / Heating

2: 100 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 24 h / Ambient temperature

With hydrogenchloride; N,N-diisopropylamine tetrazolide; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(97)10003-5