3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

Base Information

Chemical Name:3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester
CAS No.:1192322-49-8
Molecular Formula:C₂₈H₃₂O₅
Molecular Weight:448.559
Hs Code.:

Synonyms:3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

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Chemical Property of 3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

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Technology Process of 3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

There total 5 articles about 3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

: 1192322-46-5
3-(4-Hydroxyphenyl)-adamantane-1-carboxylic acid benzyl ester

: 105-39-5
chloroacetic acid ethyl ester

: 1192322-49-8
3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 828-51-3
1-Adamantanecarboxylic acid

: 1192322-49-8
3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride; bromine / 49 h / -5 - 20 °C / Inert atmosphere

2.1: aluminum (III) chloride / 24 h / -10 - 20 °C

3.1: boron tribromide / dichloromethane / 3 h / -10 - 20 °C / Inert atmosphere

4.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

4.2: 4 h / 20 - 40 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With aluminum (III) chloride; bromine; boron tribromide; potassium carbonate; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 56531-56-7
3-(4-methoxyphenyl)adamantane-1-carboxylic acid

: 1192322-49-8
3-(4-ethoxycarbonylmethoxyphenyl)adamantane-1-carboxylic acid benzylester

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron tribromide / dichloromethane / 3 h / -10 - 20 °C / Inert atmosphere

2.1: potassium hydrogencarbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 4 h / 20 - 40 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With boron tribromide; potassium carbonate; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;