methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

Base Information

Chemical Name:methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether
CAS No.:1395726-45-0
Molecular Formula:C₃₂H₃₃NO
Molecular Weight:447.62
Hs Code.:

Synonyms:methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

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Chemical Property of methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

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Technology Process of methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

There total 1 articles about methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 7507-86-0
2-bromo-5-methoxy-benzaldehyde

: 183210-84-6
1,4-bis(4-tert-butylphenyl)buta-1,3-diyne

: 1395726-45-0
methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

Guidance literature:: 2-bromo-5-methoxy-benzaldehyde; With tert-butylamine; In N,N-dimethyl-formamide; at 100 ℃; for 1h; Inert atmosphere;

1,4-bis(4-tert-butylphenyl)buta-1,3-diyne; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; lithium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 26h; Inert atmosphere;
DOI:10.1016/j.tet.2012.07.067

Reference yield: 92.0%

: 1395726-45-0
methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

: 1395728-46-7
7-iodo-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridin-3-yl methyl ether

Guidance literature:: With Iodine monochloride; In dichloromethane; acetonitrile; at 0 ℃; for 0.416667h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.07.067

Reference yield: 68.0%

: 1395726-45-0
methyl 4-(4-tert-butylphenyl)-3-[2-(4-tert-butylphenyl)ethynyl]isoquinolin-7-yl ether

: 1395727-57-7
3-methoxy-10-tert-butyl-8-(4-tert-butylphenyl)benzo[a]phenanthridine

Guidance literature:: With silver hexafluoroantimonate; (triphenylphosphine)gold(I) chloride; In toluene; at 120 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.07.067